Instrument - Chemiluminescence NO-NO2-NOx Analyzer
Short name:
NOx Box
Full name:
Chemiluminescence NO-NO2-NOx Analyzer
What is being measured:
NOx Concentrations
Sampling Protocol:
Online
Manufacturer:
Thermo Environmental
Model:
Model 42
Instrument year
:
1989
Data recording software:
Labview Program
Data analysis software:
Custom Excel Program
Raw data time resolution:
1s
Analysis data averaging:
60s
Detection limit:
0.1 ppb
Sensitivity to temperature (and correction method, if applicable):
:
N/A
Sensitivity to relative humidity (and correction method, if applicable):
:
N/A
Sampling method:
Direct gas sampling
Sample preparation method:
Filter particle contents before sampling; One of the measuring streams is flowing through catalyst system to convert NOx to NO
Sample residence time (chamber to instrument) (seconds):
Length of tubing (cm):
Instrument flow rate:
Tubing inner diameter:
1/4'' OD; 0.152'' ID
Tubing material:
FEP Teflon
Chemical identification method:
NO concentration is determined by Chemiluminescence method; NOx concentration is determined by the same method from another sample stream which flows through the catalyst box, assuming the catalyst can convert 100% of the NO2 into NO.
Data analysis method:
The raw signal is logged by the custom Labview program every second and is averaged to 1 min of the time range. Finally the data is pulled out by a custom Excel script.
Quantification method:
[NO2] = [NOx] - [NO].
Calibration method:
Standard NO and NOx gas with known concentrations was introduced into the instrument and calibration factor is calculated based on the comparison. THIS IS DONE EVERYTIME BEFORE AN EXPERIMENT.
Calibration drift estimate:
No estimate
Calibration schedule:
As Needed
Uncertainty estimation method:
N/A
Known interferences:
N/A
Link to supplemental information:
N/A
Additional notes:
N/A
Measurement uncertainty:
(a) Local_Time (N/A); (b) Experimental_Time (N/A); (c)NO_Concentration (+/- ?%); (d) NO2_Concentration (+/- ?%); (e) NOx_Concentration (+/- ?%)
Measurement units:
(a) Local_Time (N/A); (b) Experimental_Time (N/A); (c)NO_Concentration (ppb); (d) NO2_Concentration (ppb); (e) NOx_Concentration (ppb)