Instrument - Gas Chromatograph - Flame Ionization Detector
Short name:
GC-FID
Full name:
Gas Chromatograph - Flame Ionization Detector
What is being measured:
VOCs, OVOCs, IVOCs
Sampling Protocol:
Offline
Manufacturer:
Hewlett Packard
Model:
6890
Instrument year
:
None specified
Data recording software:
Agilent Chemstation 1.0
Data analysis software:
Manual Data Analysis
Raw data time resolution:
1 s
Analysis data averaging:
Detection limit:
100 pg
Sensitivity to temperature (and correction method, if applicable):
:
N/A
Sensitivity to relative humidity (and correction method, if applicable):
:
N/A
Sampling method:
Thermal desorption of Tenax adsorbent cartridges/Liquid injections
Sample preparation method:
Active sampling of adsorbent cartridges/Liquid dilutions
Sample residence time (chamber to instrument) (seconds):
Length of tubing (cm):
Instrument flow rate:
Tubing inner diameter:
Tubing material:
N/A
Chemical identification method:
Retention time matching, Kovats Retention Index
Data analysis method:
Quantification method:
Peak area is converted to concentration based on:
i) The known amount of mass added to the chamber, and the ratio of peak area before and after reaction
ii) Calibration curve of standard liquid injections
Calibration method:
Calibration of standard liquid injections are performed by adding known volumes of volumetrically prepared standards.
Calibration drift estimate:
Low (on the order of weeks)
Calibration schedule:
Uncertainty estimation method:
Uncertainty is estimated at +/- 5% due to uncertainties in sampling time for Tenax adsorbent cartridges, standard deviations of replicate measurements.
Known interferences:
Link to supplemental information:
Additional notes:
Measurement uncertainty:
(a) VOC (+/- 5%)
Measurement units:
All measurements from this instrument are converted to ppb