Instrument - Chemical Ionization - Ion Trap Mass Spectrometer
Short name:
CI-ITMS
Full name:
Chemical Ionization - Ion Trap Mass Spectrometer
What is being measured:
Fractionated organic particle extracts, gas phase extracts, derivatized compounds
Sampling Protocol:
Offline
Manufacturer:
Thermo Finnigan
Model:
PolarisQ
Instrument year
:
None specified
Data recording software:
Thermo's Xcalibur
Data analysis software:
Manual Data Analysis
Raw data time resolution:
4 Hz
Analysis data averaging:
Detection limit:
100 pg
Sensitivity to temperature (and correction method, if applicable):
:
N/A
Sensitivity to relative humidity (and correction method, if applicable):
:
N/A
Sampling method:
Direct insertion probe
Sample preparation method:
Several uL of extract containing analyte of interest is evaporated in a sample cup
Sample residence time (chamber to instrument) (seconds):
Length of tubing (cm):
Instrument flow rate:
Tubing inner diameter:
Tubing material:
Chemical identification method:
Chemical ionization using isobutane or ammonia as reagent ion. Observations of protonated parent ion, ammonia adducts, and logical neutral losses.
Data analysis method:
Quantification method:
Calibration method:
Calibration drift estimate:
No estimate
Calibration schedule:
Uncertainty estimation method:
The CI-ITMS is used as an identification, not a quantitative tool, and as such quantitative uncertainty is not reported.
Known interferences:
Link to supplemental information:
Additional notes:
Measurement uncertainty:
N/A
Measurement units:
N/A